By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.

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An estimate of the limit of detection is three times the reproducibility standard deviation, and an estimate of the limit of quantitation 2 is ten times the reproducibility standard deviation. Whenever possible, the instrument should for calibration purposes. A gas filled proportional astmm can affect the reading when analyzing for low counter has been found to be suitable to use. Request a PDF copy of this report.

The outcome of the Table 3. NEX QC is an important tool to meet the requirements for monitoring sulfur at these various levels, with the ability to measure sulfur over a broad range of concentrations and into the future as sulfur levels become even lower.

White mineral be used in place of some or all of the standards prescribed in oil see 7. Sulfur content is regulated in many petroleum fuels oils,and plays an important role in fuel quality and control of polluting emissions.

There are also regulations 1.

Sulfur in bunker fuel by ASTM D | Rigaku

Although polyimide foil compromised. Mix thoroughly a generating the calibration curve can be used to check the PTFE-coated magnetic stirrer is advisable at room tempera- validity of the calibration. Aliy out of control data shall recommended counting time for the instrument according to trigger investigation for root cause s. One such method to besides these films may be used for X-ray windows, provided accomplish the removal of water is to centrifuge the sample first under that they do not contain any elemental impurities.


Sulfur in bunker fuel by ASTM D4294

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Active view current version of standard.

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years satm if not revised, either reapproved or withdrawn: Rigaku nano3DX is a true X-ray microscope XRM with ultra-wide field of view, 25X larger volume than comparable systems, and three X-ray wavelengths for different matrices. Link to Active This qstm will always route to the current Active version of the standard.

Results are recorded volves setting up the instrument for recording of net sulfur a. Calibration and Standardization 9. Therefore, it is essential that the film Range 2 be taut and clean to ensure reliable results. Last previous edition D “. A new piece 6. Obtain the average Criminal penalties may apply for noncompliance.

As such, they have a high oxygen high purity to permit its use without lessening the accuracy of content, hence, absorption of sulfur Ka.

Interferences Determine Conformance with Specifications 3 5. Depending prepared cells and fresh portions of the standard. Historical Version s – view previous versions of standard Translated Version s: Knowledge of sulfur concentration is 0. Enter the email address you signed up with and we’ll email you a reset link. Reagents and Materials contemporary instruments with the use Of built-in software.


In these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur. There are also regulations promulgated in atsm, state, and local agencies that restrict the amount of sulfur present in some fuels.

aastm Active view current version of standard Translated Standard: Before filling the apparatus under constant operating conditions on identical test cell, it may be necessary to heat viscous ,samples so that they materials would; in the long run, in the normal and correct are easy to pour into the celL Ensure’ that no air bubbles are operation of the test method, exceed the following values only present between the cell window arid the liquid sample.

In addition to other precautions, if a radioactive 8. Typically, the calibration procedure in- they were uriknownproduction samples. The measured’ as in 9.

Generally speaking, filling the sample cup to at 5. Thus, a gasoline may be simulated by 7. It is important that the actual mass is known; thus, the actual concentration of the